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- Coulometric Karl Fischer Titrator
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Coulometric Titrator by Karl Fischer's Method PE-9210 (generator electrode with diaphragm)
7 213 $ add to cart
The price is valid for non-residents of the Russian Federation
Coulometric Titrator by Karl Fischer's Method PE-9210 is designed for fast and accurate determination of moisture content in a wide range of products and materials in the liquid phase by coulometric titration. The titrator can be used in analytical and chemical technology laboratories, in control and supervision bodies. The device is most convenient for determining moisture in crude oil, heavy petroleum products, diesel fuel, transformer oil, etc. It can be used in laboratory and industrial conditions.
Features:
- The device is listed in the State Register of Measuring Instruments of the Russian Federation under the number 55135-13;
- The diaphragm cell is the best choice when analyzing samples with a water content of up to 1000 ppm. This design is recommended for the analysis of diesel fuels, transformer and turbine oils for the most accurate and reliable determination of moisture and minimizing the occurrence of side processes;
- The metal case, painted with chemically resistant paint, reliably protects the device from external influences
- Adaptive titration algorithm guarantees high accuracy when titrating samples with low moisture content
- The Windows Embedded Compact 7 operating system installed on the device allows you to save data in the usual Word and Excel formats;
- Graphical representation of the titration process;
- Built-in methodology for getting started quickly;
- The titration is started by pressing one button;
- Creation and storage of user's techniques in memory (up to 100 techniques);
- Storing measurement results in memory (up to 1000 series);
- Accounting for the reagent resource;
- RS-232/485 port for connecting scales and controlling external devices;
- 2 USB B ports for connection to a computer, laser printer, peripheral input devices (keyboard, mouse);
- The ability to use a USB flash drive (USB flash drive) to transfer and store data;
- Prompt, high-quality and inexpensive service support for our users;
Supported standards (GOST, ASTM):
1) ISO 12937:2000 "Petroleum products. Determination of the water content. Karl Fischer coulometric titration method"
2) GOST R 54284-2010 "Crude oils. Determination of water by coulometric titration according to Karl Fischer"
3) ASTM D 4928-00 (2010) "Standard Method for the Determination of Water in Oil by Coulometric Titration according to Karl Fischer"
4) GOST R 54281-2010 "Petroleum products, lubricating oils and additives. Method for determining water by coulometric titration according to Karl Fischer"
5) GOST R IEC 60814 "Determination of moisture in liquid and solid dielectrics by coulometric titration using an automatic Karl Fischer titrator"
6) GOST R 56340-2015 "Organic liquids. Determination of water by coulometric titration according to Karl Fischer"
7) GOST 24614-81 "Liquids and gases that do not interact with the Fischer reagent. Coulometric method for determining water"
8) GOST EN 13466-1-2013 "Fertilizers. Determination of water content (Karl Fischer methods)"
9) GOST 14870-77 "Chemical products. Methods for determining water"
10) ASTM D 1533-00 «Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration»
11) ASTM E 1064-05 «Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
Technical specifications:
- The volume of the titration cell is 280 ml;
- Iodine generation in the cell - current pulses of fixed duration with an amplitude up to 2000 mA;
- Indication of the end point of titration - alternating current polarization potential;
- Determination of the end point of titration - by relative drift, by absolute drift or by time;
- The measurement range of the mass of water in the analyzed sample is from 0.01 to 200 mg;
- The limit of permissible relative error is ± 3.0%;
- The limit of the permissible relative COE of the random component of the error is 1.5%;
- Sensitivity - 0.1 micrograms of H2O;
- Indication - drift, potential, titration time, mixing speed;
- Calculations:
a) Automatic calculation of moisture content in ppm, %, mg, mcg;
b) Automatic drift compensation;
c) Taking into account the result of titration of the blank sample;
d) Statistical processing of the results of a series of measurements;
- Agitator - 100-1000 rpm, speed stabilization, step adjustment;
- Power supply:
Voltage: 198-242 Volts, 50 Hz;
Power consumption: no more than 170 watts;
- Overall dimensions:
height - no more than 200 mm;
length - no more than 350 mm;
width - no more than 275 mm;
- The weight of the titrator is not more than 6.5 kg;
- Service life - 10 years;
- The average operating time is 10,000 hours.
Transport dimensions:
1 box, 350x300x500, weight 8 kg
Basic equipment:
- Fischer titrator – 1 pc.;
- Titrator cell with generator and indicator electrodes – 1 pc.;
- Molecular sieves – 100 g.;
- Desiccant tube – 1 pc.;
- Anchor for built–in magnetic stirrer - 1 pc.;
- Connecting cables – 1 set;
- Power cable (with grounding) – 1 pc.;
- Needles (for syringe G21) 80 mm – 3 pcs.;
- Sealing lubricant - 10 g;
- Septa – 50 pcs.;
- Operating manual with verification procedure
- Certificate of verification.